Microstructural Characterization of Materials David Brandon and Wayne D. Kaplan Technion, Israel Institute of Technology Israel The internal microstructure and the microstructural features of materials are of key importance when analysing a material for a given engineering application. In specifying the internal microstructure of a material the chemistry, the crystallography, and the structural morphology need to be considered. For each of these aspects, there are three equally important stages of investigation - specimen preparation, image observation and recording, and the analysis and interpretation of recorded data. Microstructural Characterization of Matenals is an integrated treatment of the science of microstructural characterization which emphasizes the interaction of the specimen with the radiation used to probe the microstructure. The three main aspects of microstructural morphology, phase identification and crystallography, and microanalysis of the chemical composition are all covered in detail. Following an introductory chapter, the principal methods of characterization which are commonly available in a well-equipped laboratory are treated in full. These include diffraction analysis, optical microscopy, electron microscopy, and chemical microanalytical techniques. Microstructural Characterization of Materials will be of great value to both undergraduate and graduate students and includes suitable problems for students exercises. More advanced researchers will also find it highly useful as a general reference source.

Microstructural characterization is usually achieved by allowing some form of probe to interact with a carefully prepared specimen. The most commonly used probes are visible light, X-ray radiation, a high-energy electron beam, or a sharp, flexible needle. These four types of probe form the basis for optical microscopy, X-ray diffraction, electron microscopy, and scanning probe microscopy. Microstructural Characterization of Materials, 2nd Edition is an introduction to the expertise involved in assessing the microstructure of engineering materials and to the experimental methods used for this purpose. Similar to the first edition, this 2nd edition explores the methodology of materials characterization under the three headings of crystal structure, microstructural morphology, and microanalysis. The principal methods of characterization, including diffraction analysis, optical microscopy, electron microscopy, and chemical microanalytical techniques are treated both qualitatively and quantitatively. An additional chapter has been added to the new edition to cover surface probe microscopy, and there are new sections on digital image recording and analysis, orientation imaging microscopy, focused ion-beam instruments, atom-probe microscopy, and 3-D image reconstruction. As well as being fully updated, this second edition also includes revised and expanded examples and exercises, with a solutions manual available at http://develop.wiley.co.uk/microstructural2e/ Microstructural Characterization of Materials, 2nd Edition will appeal to senior undergraduate and graduate students of material science, materials engineering, and materials chemistry, as well as to qualified engineers and more advanced researchers, who?will find the book a useful and comprehensive general reference source.

This book covers mechanical, chemical and physical methods and offers introductions to surface science and the mechanics of joints. It also provides an excellent grounding in areas of materials science.