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Tables of Contents for Organic Structures from Spectra
Chapter/Section Title
Page #
Page Count
Preface
vii
Introduction
1
5
General Principles of Absorption Spectroscopy
1
2
Chromophores
3
1
Connectivity
3
1
Sensitivity
4
1
Practical Considerations
4
2
Ultraviolet (UV) Spectroscopy
6
7
Basic Instrumentation
6
1
The Nature of Ultraviolet Spectroscopy
7
1
Quantitative Aspects of Ultraviolet Spectroscopy
7
1
Classification of UV Absorption Bands
8
1
Special Terms in Ultraviolet Spectroscopy
9
1
Important UV Chromophores
9
3
The Effect of Solvents
12
1
Infrared (IR) Spectroscopy
13
5
Absorption Range and The Nature of IR Absorption
13
1
Experimental Aspects of Infrared Spectroscopy
13
1
General Features of Infrared Spectra
14
1
Important IR Chromophores
15
3
Mass Spectrometry
18
11
Ionization Processes
18
1
Instrumentation
19
1
Mass Spectral Data
20
4
Representation of Fragmentation Processes
24
1
Factors Governing Fragmentation Processes
25
1
Examples of Common Types of Fragmentation Processes
25
4
Nuclear Magnetic Resonance (NMR) Spectroscopy
29
28
The Physics of Nuclear Spins and NMR Instrumentation
29
5
The Larmor Equation and Nuclear Magnetic Resonance
29
3
Nuclear Relaxation
32
1
The Acquisition of An NMR spectrum
33
1
Continuous Wave (CW) NMR Spectroscopy
34
1
Fourier-Transform (FT) NMR Spectroscopy
35
2
Chemical Shifts in 1H NMR Spectroscopy
37
4
Spin-Spin Coupling in 1H NMR Spectroscopy
41
4
Analysis of 1H NMR Spectra
45
2
Rules for Spectral Analysis
47
10
Splitting Diagrams
49
3
Spin Decoupling
52
1
Correlation of 1H - 1H Coupling Constants with Structure
53
4
13C NMR Spectroscopy
57
7
Coupling and Decoupling in 13C NMR Spectra
57
2
Determining 13C Signal Multiplicity Using Dept
59
3
Shielding and Characteristic Chemical Shifts in 13C NMR Spectra
62
2
Miscellaneous Topics
64
8
Dynamic Processes in NMR Spectroscopy - The NMR Timescale
64
3
The Nuclear Overhauser Effect (NOE)
67
1
Advanced Techniques
68
3
The NMR Spectra of ``Other Nuclei''
71
1
Solvent - Induced Shifts
71
1
Determining the Structure of Organic Compounds from Spectra
72
3
Problems
75
Appendix
A1
Index